Synthesis and Stoichiometric Analysis of Glycine-Urea Assisted Synthesis of Nanoporous LiFePO4 /C Composite Cathodes for EES Applications.
Subhashini.Vedala1, M. Sushama2

1Dr. M.Sushama, Professor & Head, Department of Electrical & Electronics Engineering, JNTUH College of Engineering, Kukatpally, Hyderabad (Telangana,) India.
2Ms. Subhashini Vedala, Research Scholar, Department of Electrical & Electronics Engineering, Jawaharlal Nehru Technological University, Hyderabad (Telangana,) India.
Manuscript received on 07 March 2019 | Revised Manuscript received on 20 March 2019 | Manuscript published on 30 March 2019 | PP: 780-783 | Volume-8 Issue-5, March 2019 | Retrieval Number: D2822028419/19©BEIESP
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Abstract: The present research work, An economical and novel method for synthesis of LiFePO4 /C Nano composite by glycine , urea assisted combustion method with fuel to oxidizer ratio Ψ = one .The average crystallite size of obtained LiFePo4 /C composite from x-ray diffraction is 39-44nm. Morphological studies were done using scanning electron microscope the structure of the as synthesized nano material were investigated by Raman spectroscopy. The structure of the material at the molecular size scale has been investigated by FTIR transmittance and Thermal Analysis and stoichiometry analysis for Fuel to nitrate ratio for urea and glycine and for various molarities and there balancing equations and calculation for Enthalpy of combustion and adiabatic flame temperature results were presented in this paper.
Keyword: X-Ray Diffraction Analysis (XRD), Solution Combustion Synthesis, Scanning Electron Microscopy (SEM), Raman spectrum.
Scope of the Article: RFID Network and Applications